((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

Base Information

Chemical Name:((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol
CAS No.:676233-76-4
Molecular Formula:C₁₅H₁₉N₃O₅
Molecular Weight:321.333
Hs Code.:

Synonyms:((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

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Technology Process of ((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

There total 1 articles about ((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 676233-75-3
(2R,4aR,6S,8S,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-8-carbaldehyde

: 676233-76-4
((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

Guidance literature:: With sodium tetrahydroborate; In water; ethyl acetate;
DOI:10.1016/j.tetlet.2003.12.034

Reference yield: 92.0%

: 124-63-0
methanesulfonyl chloride

: 676233-76-4
((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

: 676233-77-5
Methanesulfonic acid (2R,4aR,6S,8R,8aS)-8-azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ylmethyl ester

Guidance literature:: With pyridine;
DOI:10.1016/j.tetlet.2003.12.034

Reference yield:

: 676233-76-4
((2R,4aR,6S,8R,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-methanol

: 98758-29-3
methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine

2: NaBH₄ / dimethylsulfoxide / 8 h / 80 °C

With pyridine; sodium tetrahydroborate; In dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2003.12.034