(Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one

Base Information

• Chemical Name: (Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one
• CAS No.: 102028-66-0
• Molecular Formula: C₁₈H₁₅NO₄
• Molecular Weight: 309.321
• Mol file: 102028-66-0.mol

Synonyms:(Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one

Chemical Property of (Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one

There total 1 articles about (Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

2-(3,4-dimethoxybenzamido)acetic acid (59893-89-9) + benzaldehyde (100-52-7) → (Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one (102028-66-0)

Guidance literature:

With sodium acetate; acetic anhydride; at 100 ℃; for 2h;

DOI:10.1039/b907647f

Reference yield: 55.0%

palladium diacetate (3375-31-3) + (Z)-2-(3,4-dimethoxyphenyl)-4-benzylidene-(4H)-1,3-oxazol-5-one (102028-66-0) + trifluoroacetic acid (76-05-1) → [Pd2(2-(3,4-dimethoxyphenyl)-4-(benzylidene-κC2)-(4H)-1,3-oxazol-5-one(1-))2(μ-trifluoroacetato)2] (1328932-59-7)

Guidance literature:

In trifluoroacetic acid; at 81°C for 3 h;

DOI:10.1021/ic200564d

Reference yield:

C6H5CH((C3NO)O)C6H3(OCH3)2 (102028-66-0) + palladium diacetate (3375-31-3) + trifluoroacetic acid (76-05-1) → Pd2[(C6H4)CH((C3NO)O)C6H3(OCH3)2]2(CF3C(O)O)2 (1328932-59-7)

Guidance literature:

In trifluoroacetic acid; reflux Pd(OAc)2 with ligand in trifluoroacetic acid;

DOI:10.1039/b907647f

upstream raw materials:

2-(3,4-dimethoxybenzamido)acetic acid

benzaldehyde

Downstream raw materials:

α-veratroylamino-trans-cinnamic acid

[Pd2(2-(3,4-dimethoxyphenyl)-4-(benzylidene-κC2)-(4H)-1,3-oxazol-5-one(1-))2(μ-trifluoroacetato)2]

Pd₂[(C₆H₄)CH((C₃NO)O)C₆H₃(OCH₃)2]2(CF₃C(O)O)2