(4S,8S)-p-mentha-1,5-dien-9-ol

Base Information

Chemical Name:(4S,8S)-p-mentha-1,5-dien-9-ol
CAS No.:1340481-21-1
Molecular Formula:C₁₀H₁₆O
Molecular Weight:152.236
Hs Code.:

Synonyms:(4S,8S)-p-mentha-1,5-dien-9-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,8S)-p-mentha-1,5-dien-9-ol

Chemical Property:

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Technology Process of (4S,8S)-p-mentha-1,5-dien-9-ol

There total 1 articles about (4S,8S)-p-mentha-1,5-dien-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1340481-27-7
(4S,8S)-p-mentha-1,5-dien-9-yl 3,5-dinitrobenzoate

: 1340481-21-1
(4S,8S)-p-mentha-1,5-dien-9-ol

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃;
DOI:10.1016/j.tetasy.2011.07.014

Reference yield:

: 1340481-21-1
(4S,8S)-p-mentha-1,5-dien-9-ol

: 1157861-49-8
(1S,4R,8S)-3-oxo-p-menthan-9-oic acid

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / diethyl ether / 20 °C

2: palladium on activated charcoal; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr

3: sodium periodate; rhodium(III) chloride hydrate; water / tetrachloromethane; acetonitrile / 20 °C

With sodium periodate; rhodium(III) chloride hydrate; palladium on activated charcoal; boron trifluoride diethyl etherate; water; hydrogen; In tetrachloromethane; diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetasy.2011.07.014

Reference yield:

: 1340481-21-1
(4S,8S)-p-mentha-1,5-dien-9-ol

: 1340481-36-8
(1S,4R,8S)-3-oxo-p-menthan-9-oic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / diethyl ether / 20 °C

2: palladium on activated charcoal; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr

3: sodium periodate; rhodium(III) chloride hydrate; water / tetrachloromethane; acetonitrile / 20 °C

4: diethyl ether / 1 h / 0 °C

With sodium periodate; rhodium(III) chloride hydrate; palladium on activated charcoal; boron trifluoride diethyl etherate; water; hydrogen; In tetrachloromethane; diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetasy.2011.07.014