1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

Base Information

Chemical Name:1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene
CAS No.:1204220-09-6
Molecular Formula:C₁₆H₁₆BrClO
Molecular Weight:342.636
Hs Code.:

Synonyms:1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

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Chemical Property of 1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

Chemical Property:

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Technology Process of 1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

There total 7 articles about 1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204220-07-4
(5-bromo-2-chloro-4-(methoxy-d3)phenyl)(4-ethylphenyl)methanone

: 1204220-09-6
1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid; at 0 - 20 ℃;

Reference yield:

: 143945-65-7
2-amino-4-fluoro-5-bromobenzoic acid

: 1204220-09-6
1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; copper(l) chloride; sodium nitrite / water / 2 h / 0 °C

1.2: 0 - 7 °C

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

3.1: triethylamine / dichloromethane / 25 °C

4.1: tetrahydrofuran / 0 - 25 °C

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

5.2: 3 h

6.1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / 0 - 20 °C

With hydrogenchloride; triethylsilane; oxalyl dichloride; trifluorormethanesulfonic acid; sodium hydride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; copper(l) chloride; sodium nitrite; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: C₇H₂BrCl₂FO

: 1204220-09-6
1-bromo-4-chloro-5-(4-ethylbenzyl)-2-(methoxy-d3)benzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 25 °C

2.1: tetrahydrofuran / 0 - 25 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3.2: 3 h

4.1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / 0 - 20 °C

With triethylsilane; trifluorormethanesulfonic acid; sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;