2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

Base Information

Chemical Name:2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole
CAS No.:110569-83-0
Molecular Formula:C₃₄H₄₄N₂O₅
Molecular Weight:560.734
Hs Code.:

Synonyms:2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

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Chemical Property of 2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

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Technology Process of 2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

There total 8 articles about 2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.1%

: 71128-83-1
2-methoxy-5-methyl-1,3-benzenedicarboxaldehyde

: 98977-16-3
<4-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>butyl>triphenylphosphonium iodide

: 110569-83-0
2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

Guidance literature:: With potassium carbonate; In 1,4-dioxane; for 45h; Heating;
DOI:10.1021/jo00233a011

Reference yield:

: 6327-85-1
2,6-bis(hydroxymethyl)-4-methyl-anisole

: 110569-83-0
2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DMSO/(COCl)2, 2.) Et₃N / 1.) methylene chloride, -78 deg C, 15 min, 2.) methylene chloride, from -78 deg C to RT

2: 47.1 percent / K₂CO₃ / dioxane / 45 h / Heating

With oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; triethylamine; In 1,4-dioxane;
DOI:10.1021/jo00233a011

Reference yield:

: 98977-10-7
4-<5-(ethoxycarbonyl)-2-carboxy-4-methylpyrrol-3-yl>-1-iodobutane

: 110569-83-0
2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaHCO₃, 2.) KI/I₂ / 1.) water, MeCl₂, reflux, 2.) water, MeCl₂, reflux, 30 min

2: 43.4 percent / HI / ethanol / 1 h

3: 86.2 percent / toluene / 19.5 h / Heating

4: 47.1 percent / K₂CO₃ / dioxane / 45 h / Heating

With hydrogen iodide; iodine; sodium hydrogencarbonate; potassium carbonate; potassium iodide; In 1,4-dioxane; ethanol; toluene;
DOI:10.1021/jo00233a011