benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

Base Information

Chemical Name:benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate
CAS No.:1356037-46-1
Molecular Formula:C₂₀H₂₄NO₇P
Molecular Weight:421.387
Hs Code.:

Synonyms:benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

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Chemical Property of benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

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Technology Process of benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

There total 5 articles about benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30379-58-9
benzyl glycolate

: 107072-65-1
C₁₁H₁₅ClNO₄P

: 1356037-46-1
benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 72h;
DOI:10.1016/j.bmcl.2011.10.094

Reference yield:

: 621-84-1
O-benzyl carbamate

: 1356037-46-1
benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 3 h / 0 - 85 °C

2: methanol / 1,4-dioxane; methanol / 12 h / 20 °C

3: water; sodium hydroxide / methanol / 5 h / 85 °C

4: thionyl chloride / chloroform / 8 h / 20 °C

5: triethylamine / chloroform / 72 h / 20 °C

With methanol; thionyl chloride; water; acetic acid; triethylamine; sodium hydroxide; In 1,4-dioxane; methanol; chloroform;
DOI:10.1016/j.bmcl.2011.10.094

Reference yield:

: 65164-80-9
diphenyl 1-(phenylmethoxycarbonylamino)ethyl phosphonate

: 1356037-46-1
benzyl {[1-(benzyloxycarbonylamino)ethyl(methoxy)phosphoryl]oxy}acetate

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 1,4-dioxane; methanol / 12 h / 20 °C

2: water; sodium hydroxide / methanol / 5 h / 85 °C

3: thionyl chloride / chloroform / 8 h / 20 °C

4: triethylamine / chloroform / 72 h / 20 °C

With methanol; thionyl chloride; water; triethylamine; sodium hydroxide; In 1,4-dioxane; methanol; chloroform;
DOI:10.1016/j.bmcl.2011.10.094