1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate

Base Information

Chemical Name:1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate
CAS No.:1191107-27-3
Molecular Formula:C₁₉H₂₆ClNO₄
Molecular Weight:367.873
Hs Code.:

Synonyms:1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate

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Chemical Property of 1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate

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Technology Process of 1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate

There total 1 articles about 1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 553631-33-7
tert-butyl 4-(3-chlorophenyl)-4-cyanopiperidine-1-carboxylate

: 64-17-5
ethanol

: 24424-99-5
di-tert-butyl dicarbonate

: 1191107-27-3
1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate

Guidance literature:: tert-butyl 4-(3-chlorophenyl)-4-cyanopiperidine-1-carboxylate; With sulfuric acid; water; for 3h; Reflux;

ethanol; In water;

di-tert-butyl dicarbonate; With triethylamine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1191107-27-3
1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate

: 954123-04-7
tert-butyl 4-(3-chlorophenyl)-4-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: 1-tert-butyl ethyl 4-(3-chlorophenyl)piperidine-1,4-dicarboxylate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

With water; sodium sulfate; Saturated solution;