cyclohex-2-enyl 4-(tosyloxy)benzoate

Base Information

Chemical Name:cyclohex-2-enyl 4-(tosyloxy)benzoate
CAS No.:1345403-81-7
Molecular Formula:C₂₀H₂₀O₅S
Molecular Weight:372.442
Hs Code.:

Synonyms:cyclohex-2-enyl 4-(tosyloxy)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohex-2-enyl 4-(tosyloxy)benzoate

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Technology Process of cyclohex-2-enyl 4-(tosyloxy)benzoate

There total 2 articles about cyclohex-2-enyl 4-(tosyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 51804-15-0
4-carboxyphenyl 4-methylbenzenesulfonate

: 110-83-8
cyclohexene

: 1345403-81-7
cyclohex-2-enyl 4-(tosyloxy)benzoate

Guidance literature:: With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In benzene; at 80 ℃; for 8h;
DOI:10.1021/ol3013606

Reference yield:

: 80459-48-9
4-tosyloxybenzaldehyde

: 1345403-81-7
cyclohex-2-enyl 4-(tosyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide / water / 24 h / 40 °C

2: copper(I) bromide / dichloromethane; water / 36 h / 40 °C

With tetra-(n-butyl)ammonium iodide; copper(I) bromide; In dichloromethane; water; 2: Kharasch-Sosnovsky reaction;
DOI:10.1039/c1cc14602e