1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

Base Information

Chemical Name:1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate
CAS No.:1617534-62-9
Molecular Formula:C₂₅H₁₈O₃
Molecular Weight:366.416
Hs Code.:

Synonyms:1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

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Technology Process of 1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

There total 2 articles about 1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 66-77-3
1-naphthaldehyde

: 134-81-6
benzil

: 1617534-62-9
1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 50 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c4ob00759j

Reference yield:

: 1459-20-7
1,2-diphenyl-2-oxoethyl benzoate

: 1617534-62-9
1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid; acetic acid; ammonium nitrate / 2 h / 150 °C / Microwave irradiation; Sealed tube

2: potassium tert-butylate / dimethyl sulfoxide / 50 °C / Inert atmosphere

With ammonium nitrate; potassium tert-butylate; acetic acid; trifluoroacetic acid; In dimethyl sulfoxide; 2: |Benzoin Condensation;
DOI:10.1039/c4ob00759j

Reference yield: 98.0%

: 1617534-62-9
1-(naphthalen-1-yl)-2-oxo-2-phenylethyl benzoate

: 16216-08-3
2-(naphthalen-1-yl)-1-phenylethan-1-one

Guidance literature:: With palladium(II) trifluoroacetate; hydrogen; [(4S)-4-[5-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphanyl-1,3-benzodioxol-4-yl]-4,5,6,7-tetrahydro-1,3-benzodioxol-5-yl]-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphane; In acetone; at 60 ℃; for 48h; under 45004.5 Torr; chemoselective reaction; Glovebox; Autoclave;
DOI:10.1002/anie.201603590