Technology Process of C29H30N8O2
There total 9 articles about C29H30N8O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 1.5h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere
1.2: 2 h / 0 - 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / 18 h / 125 °C
3.1: 2,2,2-trifluoroethanol / 1.5 h / 120 - 140 °C / Microwave irradiation
4.1: iron; ammonium chloride / water; ethanol / 4 h / Reflux
5.1: zinc; tris-(dibenzylideneacetone)dipalladium(0); XPhos / N,N-dimethyl acetamide / 2 h / 95 °C / Inert atmosphere
6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / Cooling with ice
With
tris-(dibenzylideneacetone)dipalladium(0); iron; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; zinc; XPhos;
In
tetrahydrofuran; ethanol; dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl acetamide; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / 18 h / 125 °C
2: 2,2,2-trifluoroethanol / 1.5 h / 120 - 140 °C / Microwave irradiation
3: iron; ammonium chloride / water; ethanol / 4 h / Reflux
4: zinc; tris-(dibenzylideneacetone)dipalladium(0); XPhos / N,N-dimethyl acetamide / 2 h / 95 °C / Inert atmosphere
5: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / Cooling with ice
With
tris-(dibenzylideneacetone)dipalladium(0); iron; ammonium chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; zinc; XPhos;
In
ethanol; dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl acetamide; water;