3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

Base Information

Chemical Name:3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin
CAS No.:161822-09-9
Molecular Formula:C₅₂H₉₃N₇O₂₁
Molecular Weight:1152.34
Hs Code.:

Synonyms:3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

Chemical Property:

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Technology Process of 3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

There total 1 articles about 3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 147920-22-7
2''-amino-2''-deoxyarbekacin

: 161822-09-9
3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

Guidance literature:: With triethylamine; In 1,4-dioxane; methanol; water; at 35 ℃; for 26h;
DOI:10.7164/antibiotics.47.821

Reference yield: 91.0%

: 108-24-7
acetic anhydride

: 161822-09-9
3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

: 161822-10-2
4'',6'',2'''-tri-O-acetyl-3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

Guidance literature:: With pyridine; for 3h; Ambient temperature;
DOI:10.7164/antibiotics.47.821

Reference yield:

: 161822-09-9
3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-2''-deoxyarbekacin

: 3,2',6',3'',4'''-pentakis(N-tert-butoxycarbonyl)-2''-(tert-butoxycarbonyl)amino-6''-chloro-2'',6''-dideoxyarbekacin

Guidance literature:: With pyridine; 1H-imidazole; tetrachloromethane; triphenylphosphine; In acetonitrile; at 65 ℃; for 5h;
DOI:10.7164/antibiotics.47.821