C₂₂H₃₁IO₆

Base Information

Chemical Name:C₂₂H₃₁IO₆
CAS No.:1256633-60-9
Molecular Formula:C₂₂H₃₁IO₆
Molecular Weight:518.389
Hs Code.:

C<sub>22</sub>H<sub>31</sub>IO<sub>6</sub>

Synonyms:C₂₂H₃₁IO₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₁IO₆

Chemical Property:

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Technology Process of C₂₂H₃₁IO₆

There total 3 articles about C₂₂H₃₁IO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1256633-59-6
(2S,5R,6E,8E)-1-(3,4-dimethoxybenzyloxy)-5-hydroxy-9-iodo-2-methylnona-6,8-dien-3-one

: 123-38-6
propionaldehyde

: 1256633-60-9
C₂₂H₃₁IO₆

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at -20 ℃; for 0.75h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol102425n

Reference yield:

: 1256633-53-0
C₁₄H₂₀O₄

: 1256633-60-9
C₂₂H₃₁IO₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

1.2: 16.5 h / -78 - -20 °C / Inert atmosphere

2.1: samarium diiodide / tetrahydrofuran / 0.75 h / -20 °C / Inert atmosphere

With samarium diiodide; triethylamine; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; diethyl ether; 2.1: Evans-Tishchenko reduction;
DOI:10.1021/ol102425n

Reference yield:

: 168295-35-0
(2E,4E)-5-iodopenta-2,4-dienal

: 1256633-60-9
C₂₂H₃₁IO₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

1.2: 16.5 h / -78 - -20 °C / Inert atmosphere

2.1: samarium diiodide / tetrahydrofuran / 0.75 h / -20 °C / Inert atmosphere

With samarium diiodide; triethylamine; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; diethyl ether; 2.1: Evans-Tishchenko reduction;
DOI:10.1021/ol102425n