C₃₅H₂₈N₄O₁₀

Base Information

• Chemical Name: C₃₅H₂₈N₄O₁₀
• CAS No.: 1346550-28-4
• Molecular Formula: C₃₅H₂₈N₄O₁₀
• Molecular Weight: 664.628
• Mol file: 1346550-28-4.mol

Synonyms:C₃₅H₂₈N₄O₁₀

Chemical Property of C₃₅H₂₈N₄O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₈N₄O₁₀

There total 3 articles about C₃₅H₂₈N₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

C25H19N3O4 (1346550-27-3) + nitroveratryloxycarbonyl chloride (42855-00-5) → C35H28N4O10 (1346550-28-4)

Guidance literature:

With diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/cb2002889

Reference yield:

3',6'-diamino-spiro[phthalan-1,9'-xanthen]-3-one (509-72-8) → C35H28N4O10 (1346550-28-4)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide

2: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

3: trifluoroacetic acid / dichloromethane

4: diisopropylamine / N,N-dimethyl-formamide

With diphenyl phosphoryl azide; sodium hydride; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/cb2002889

Reference yield:

3'-amino-6'-(tert-butoxycarbonylamino)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one (897929-08-7) → C35H28N4O10 (1346550-28-4)

Guidance literature:

Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

2: trifluoroacetic acid / dichloromethane

3: diisopropylamine / N,N-dimethyl-formamide

With diphenyl phosphoryl azide; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/cb2002889

upstream raw materials:

3'-amino-6'-(tert-butoxycarbonylamino)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one

C₂₅H₁₉N₃O₄

nitroveratryloxycarbonyl chloride

3',6'-diamino-spiro[phthalan-1,9'-xanthen]-3-one