[Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃)

Base Information

• Chemical Name: [Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃)
• CAS No.: 1073131-16-4
• Molecular Formula: CF₃O₃S*C₂₅H₂₈N₂PPdS
• Molecular Weight: 675.041

Synonyms:[Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃)

Chemical Property of [Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃)

Chemical Property:

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Technology Process of [Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃)

There total 1 articles about [Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-[(diphenylphosphino)methyl]thiazoline (954372-65-7) + bis[(benzyldimethylamino)chloropalladium(II)] + silver trifluoromethanesulfonate (2923-28-6) → [Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO3CF3) (1073131-16-4)

Guidance literature:

In tetrahydrofuran; under N2; solid AgSO3CF3 added to soln. of Pd complex in THF; filtered into soln. of ligand in THF; stirred at room temp. overnight; vol. reduced under vac.; pentane added; ppt. washed with pentane; dried in vac.; elem. anal.;

DOI:10.1021/ic800934h

Reference yield: 97.7%

[Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO3CF3) (1073131-16-4) → [Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)] (1073131-17-5)

Guidance literature:

With t-BuOK; In tetrahydrofuran; byproducts: KOSO2CF3; under N2; t-BuOK added to soln. of Pd complex in THF; stirred overnight; filtered; filtrate taken to dryness; extd. with toluene; extract concd. under vac.; pentane added; ppt. collected; elem. anal.;

DOI:10.1021/ic800934h

upstream raw materials:

2-[(diphenylphosphino)methyl]thiazoline

silver trifluoromethanesulfonate

Downstream raw materials:

[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

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