N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

Base Information

Chemical Name:N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide
CAS No.:145942-09-2
Molecular Formula:C₁₃H₁₆F₂N₄O₃S
Molecular Weight:346.358
Hs Code.:

Synonyms:N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

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Chemical Property of N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

Chemical Property:

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Technology Process of N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

There total 3 articles about N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 145942-08-1
N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4-(1H-1,2,4-triazol-1-yl)-2-butane]sulfenamide

: 145942-09-2
N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

Guidance literature:: With potassium permanganate; In acetone; Ambient temperature;
DOI:10.1248/cpb.42.85

Reference yield:

: 136598-92-0
bis<(1R,2R)-2-(2,4-difluorophenyl)-2-hydroxy-1-methyl-3-(1H-1,2,4-triazol-1-yl)propyl> disulfide

: 145942-09-2
N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂ / CH₂Cl₂; CCl₄ / 0.33 h / 0 °C

2: CH₂Cl₂; CCl₄; toluene / 0.5 h / 0 °C

3: aq. KMnO₄ / acetone / Ambient temperature

With potassium permanganate; chlorine; In tetrachloromethane; dichloromethane; acetone; toluene;
DOI:10.1248/cpb.42.85

Reference yield:

: 1026878-17-0
C₁₂H₁₂ClF₂N₃OS

: 145942-09-2
N-methyl-[(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4(1H-1,2,4-triazol-1-yl)-2-butane]sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂; CCl₄; toluene / 0.5 h / 0 °C

2: aq. KMnO₄ / acetone / Ambient temperature

With potassium permanganate; In tetrachloromethane; dichloromethane; acetone; toluene;
DOI:10.1248/cpb.42.85