ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride

Base Information

Chemical Name:ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride
CAS No.:237748-28-6
Molecular Formula:C₁₂H₂₃B₁₀NO₂*ClH
Molecular Weight:357.891
Hs Code.:

Synonyms:ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride

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Chemical Property of ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride

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Technology Process of ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride

There total 1 articles about ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 185247-48-7
3-[1,2-dicarba-closo-dodecacarboranyl(methyleneoxy)]benzonitrile

: 237748-28-6
ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride

Guidance literature:: In ethanol; bubbling dry HCl through soln. of carborane derivative (45 min), stirring (overnight); evapn., crystn., trituration (Et2O), filtration (under N2);
DOI:10.1071/C98148

Reference yield: 51.0%

: 237748-28-6
ethyl 3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]benzenecarboximidate hydrochloride

: 23491-49-8
4-<5'-(4''-methylpiperazin-1''-yl)benzimidazol-2'-yl>benzene-1,2-diamine

: 237748-24-2
3-[(1,2-dicarba-closo-dodecaboranyl)methoxy]-1-[5'-[5''-(4-methylpiperazin-1'''-yl)benzimidazol-2''-yl]benzimidazol-2'-yl]benzene

Guidance literature:: In ethanol; acetic acid; N2 atmosphere; refluxing (4.5 h); pptn. on cooling (fridge, 3 h), filtration, washing (glacial HOAc/EtOH, then Et2O), drying (vac.);
DOI:10.1071/C98148