phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

Base Information

Chemical Name:phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate
CAS No.:1300090-45-2
Molecular Formula:C₃₁H₂₃N₅O₅
Molecular Weight:545.554
Hs Code.:

Synonyms:phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

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Chemical Property of phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

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Technology Process of phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

There total 5 articles about phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49615-93-2
(3-aminobenzo[b]furan-2-yl)phenylmethanone

: 124676-19-3
2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine

: 1300090-45-2
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

Guidance literature:: 2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine; With oxalyl dichloride; dmap; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;

(3-aminobenzo[b]furan-2-yl)phenylmethanone; With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

: 49615-93-2
(3-aminobenzo[b]furan-2-yl)phenylmethanone

: 517874-18-9
(Benzotriazol-1-yl-chlorocarbonyl-methyl)-carbamic acid benzyl ester

: 1300090-45-2
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1300090-45-2
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 18 h / 60 °C / Inert atmosphere

2: 4-methyl-morpholine / tetrahydrofuran / 18 h / 20 °C

With 4-methyl-morpholine; potassium carbonate; In tetrahydrofuran; acetone;