phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

Base Information

Chemical Name:phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate
CAS No.:1300090-01-0
Molecular Formula:C₂₅H₁₉N₃O₄
Molecular Weight:425.444
Hs Code.:

Synonyms:phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

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Chemical Property of phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

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Technology Process of phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

There total 5 articles about phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1300090-45-2
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate

: 1300090-01-0
phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

Guidance literature:: phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-oxo-2-{[2-(phenyl carbonyl)-1-benzofuran-3-yl]amino}ethyl)carbamate; With ammonia; In methanol; at 20 ℃; for 4h; Inert atmosphere;

With acetic acid; In methanol; for 48h;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1300090-01-0
phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 18 h / 60 °C / Inert atmosphere

2.1: 4-methyl-morpholine / tetrahydrofuran / 18 h / 20 °C

3.1: ammonia / methanol / 4 h / 20 °C / Inert atmosphere

3.2: 48 h

With 4-methyl-morpholine; ammonia; potassium carbonate; In tetrahydrofuran; methanol; acetone;

Reference yield:

: 611-20-1
salicylonitrile

: 1300090-01-0
phenylmethyl (2-oxo-5-phenyl-2,3-dihydro-1H-[1]benzofuro[3,2-e][1,4]diazepin-3-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 18 h / 60 °C / Inert atmosphere

2.1: 4-methyl-morpholine / tetrahydrofuran / 18 h / 20 °C

3.1: ammonia / methanol / 4 h / 20 °C / Inert atmosphere

3.2: 48 h

With 4-methyl-morpholine; ammonia; potassium carbonate; In tetrahydrofuran; methanol; acetone;