methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

Base Information

Chemical Name:methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate
CAS No.:131516-24-0
Molecular Formula:C₂₄H₂₅NO₆
Molecular Weight:423.466
Hs Code.:

Synonyms:methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

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Technology Process of methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

There total 9 articles about methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 131516-23-9
4-(2-hydroxyphenyl)-6-methoxy-5-methyl-2-phenylpyridine-3-carboxylic acid

: 107-30-2
chloromethyl methyl ether

: 131516-24-0
methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

Guidance literature:: With sodium hydride; N,N-dimethyl-formamide; 1) 0 deg C to 25 deg C, 10 min, 2) 45 min;
DOI:10.1021/jo00002a077

Reference yield:

: 1846-74-8
3-benzoyl-chromen-2-one

: 131516-24-0
methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: HONH₂*HCl, pyridine / ethanol

2: 75 percent / triethylamine / CCl₄ / 1) 2 deg C, 15 min, 2) 25 deg C, 1 h

3: benzene / 2 h / 25 °C

4: potassium tert-butoxide / tetrahydrofuran / 1 h / -30 °C

5: 91 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 1 h / 25 °C

6: 95 percent / 4 N aq. LiOH / tetrahydrofuran / 1 h / 25 °C

7: 95 percent / DMF, NaH / 1) 0 deg C to 25 deg C, 10 min, 2) 45 min

With pyridine; lithium hydroxide; hydroxylamine hydrochloride; potassium tert-butylate; sodium hydride; triethylamine; N,N-dimethyl-formamide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; benzene;
DOI:10.1021/jo00002a077

Reference yield:

: 118922-26-2
3-(α-hydroxyimino-benzyl)-coumarin

: 131516-24-0
methoxymethyl 6-methoxy-4-<2-<(methoxymethyl)oxy>phenyl>-5-methyl-2-phenylpyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / triethylamine / CCl₄ / 1) 2 deg C, 15 min, 2) 25 deg C, 1 h

2: benzene / 2 h / 25 °C

3: potassium tert-butoxide / tetrahydrofuran / 1 h / -30 °C

4: 91 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 1 h / 25 °C

5: 95 percent / 4 N aq. LiOH / tetrahydrofuran / 1 h / 25 °C

6: 95 percent / DMF, NaH / 1) 0 deg C to 25 deg C, 10 min, 2) 45 min

With lithium hydroxide; potassium tert-butylate; sodium hydride; triethylamine; N,N-dimethyl-formamide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; tetrachloromethane; dichloromethane; benzene;
DOI:10.1021/jo00002a077