4-chloro-N-[2-({2-[(4-methoxybenzyl)amino]-2-oxoethyl}sulfanyl)-1,3-benzothiazol-6-yl]benzamide

Base Information

Chemical Name:4-chloro-N-[2-({2-[(4-methoxybenzyl)amino]-2-oxoethyl}sulfanyl)-1,3-benzothiazol-6-yl]benzamide
CAS No.:532421-08-2
Molecular Formula:C₂₄H₂₀ClN₃O₃S₂
Molecular Weight:498.026
Hs Code.:
Mol file:532421-08-2.mol

Synonyms:4-chloro-N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

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Chemical Property of 4-chloro-N-[2-({2-[(4-methoxybenzyl)amino]-2-oxoethyl}sulfanyl)-1,3-benzothiazol-6-yl]benzamide

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Technology Process of 4-chloro-N-[2-({2-[(4-methoxybenzyl)amino]-2-oxoethyl}sulfanyl)-1,3-benzothiazol-6-yl]benzamide

There total 3 articles about 4-chloro-N-[2-({2-[(4-methoxybenzyl)amino]-2-oxoethyl}sulfanyl)-1,3-benzothiazol-6-yl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532422-39-2
C₁₇H₁₇N₃O₂S₂

: 122-01-0
4-chloro-benzoyl chloride

: 532421-08-2
4-chloro-N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/j.bmcl.2010.12.124

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 532421-08-2
4-chloro-N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dichloromethane / 0 °C / Reflux

2: potassium carbonate / acetone / 4 h / Reflux

3: sodium hydrogencarbonate / dichloromethane / 6 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2010.12.124

Reference yield:

: 81494-05-5
2-chloro-N-(4-methoxybenzyl)acetamide

: 532421-08-2
4-chloro-N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 4 h / Reflux

2: sodium hydrogencarbonate / dichloromethane / 6 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2010.12.124