C₁₇H₁₄Br₂O₄

Base Information

Chemical Name:C₁₇H₁₄Br₂O₄
CAS No.:1400055-39-1
Molecular Formula:C₁₇H₁₄Br₂O₄
Molecular Weight:442.104
Hs Code.:

C<sub>17</sub>H<sub>14</sub>Br<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₇H₁₄Br₂O₄

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Chemical Property of C₁₇H₁₄Br₂O₄

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Technology Process of C₁₇H₁₄Br₂O₄

There total 4 articles about C₁₇H₁₄Br₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1400055-34-6
C₁₆H₁₂Br₂O₃

: 149-73-5
trimethyl orthoformate

: 1400055-39-1
C₁₇H₁₄Br₂O₄

Guidance literature:: With formic acid; sulfuric acid; bis-[(trifluoroacetoxy)iodo]benzene; at 23 ℃; for 12h; Cooling with ice; Inert atmosphere;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 74003-55-7
3,4-dibromobenzaldehyde

: 1400055-39-1
C₁₇H₁₄Br₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

3.1: bis-[(trifluoroacetoxy)iodo]benzene; formic acid; sulfuric acid / 12 h / 23 °C / Cooling with ice; Inert atmosphere

With 9-O-benzylcupreidine; formic acid; sulfuric acid; piperdinium acetate; bis-[(trifluoroacetoxy)iodo]benzene; In toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 1351365-53-1
C₁₄H₁₈O₅

: 1400055-39-1
C₁₇H₁₄Br₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

3.1: bis-[(trifluoroacetoxy)iodo]benzene; formic acid; sulfuric acid / 12 h / 23 °C / Cooling with ice; Inert atmosphere

With 9-O-benzylcupreidine; formic acid; sulfuric acid; piperdinium acetate; bis-[(trifluoroacetoxy)iodo]benzene; In toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r