6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

Base Information

Chemical Name:6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol
CAS No.:147807-86-1
Molecular Formula:C₁₆H₂₇NO₅
Molecular Weight:313.394
Hs Code.:

Synonyms:6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

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Chemical Property of 6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

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Technology Process of 6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

There total 9 articles about 6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 147807-85-0
2-amino>acetaldehyde diethyl acetal

: 147807-86-1
6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 3040 Torr;

Reference yield:

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

: 147807-86-1
6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

Guidance literature:: Multi-step reaction with 8 steps

1: 1) BuLi, tetramethylethylenediamine / 1) hexane, room temperature, 24 h

2: 77 percent / NaH, PrSH / dimethylformamide / 1 h / 90 °C

3: 94 percent / K₂CO₃ / ethanol / Heating

4: 100 percent / Bu₄NI, 50percent aq. NaOH / CH₂Cl₂ / 6 h / Heating

5: 66 percent / NaOCH₂Ph / 100 °C

6: 80 percent / pyridinium chlorochromate on Al₂O₃, NaOAc / CH₂Cl₂ / Heating

7: 95 percent / NaCNBH₃, AcOH, MgSO₄ / ethanol / Heating

8: 93 percent / H₂ / 10percent Pd-C / methanol / 3040 Torr

With sodium hydroxide; n-butyllithium; 1-thiopropane; N,N,N,N,-tetramethylethylenediamine; pyridiniumchlorochromate on aluminumoxide; hydrogen; sodium acetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; magnesium sulfate; potassium carbonate; acetic acid; sodium phenyl-methanolate; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 147807-80-5
2?hydroxy?3?methoxy?4?methylbenzaldehyde

: 147807-86-1
6-[1-(2,2-Diethoxy-ethylamino)-2-hydroxy-ethyl]-2-methoxy-3-methyl-phenol

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / K₂CO₃ / ethanol / Heating

2: 100 percent / Bu₄NI, 50percent aq. NaOH / CH₂Cl₂ / 6 h / Heating

3: 66 percent / NaOCH₂Ph / 100 °C

4: 80 percent / pyridinium chlorochromate on Al₂O₃, NaOAc / CH₂Cl₂ / Heating

5: 95 percent / NaCNBH₃, AcOH, MgSO₄ / ethanol / Heating

6: 93 percent / H₂ / 10percent Pd-C / methanol / 3040 Torr

With sodium hydroxide; pyridiniumchlorochromate on aluminumoxide; hydrogen; sodium acetate; tetra-(n-butyl)ammonium iodide; sodium cyanoborohydride; magnesium sulfate; potassium carbonate; acetic acid; sodium phenyl-methanolate; palladium on activated charcoal; In methanol; ethanol; dichloromethane;