C₁₈H₁₇N₃O₂*ClH

Base Information

Chemical Name:C₁₈H₁₇N₃O₂*ClH
CAS No.:1616930-42-7
Molecular Formula:C₁₈H₁₇N₃O₂*ClH
Molecular Weight:343.813
Hs Code.:

C<sub>18</sub>H<sub>17</sub>N<sub>3</sub>O<sub>2</sub>*ClH

Synonyms:C₁₈H₁₇N₃O₂*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₇N₃O₂*ClH

Chemical Property:

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Technology Process of C₁₈H₁₇N₃O₂*ClH

There total 7 articles about C₁₈H₁₇N₃O₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 67-56-1
methanol

: 1616930-41-6
C₁₇H₁₅N₃O₂

: 1616930-42-7
C₁₈H₁₇N₃O₂*ClH

Guidance literature:: With thionyl chloride; for 1h; Reflux;

Reference yield:

: 156001-51-3
3-Bromo-6-methyl-benzonitrile

: 1616930-42-7
C₁₈H₁₇N₃O₂*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium / diethyl ether / 2 h / 20 °C

1.2: 4 h / Reflux

2.1: ethanol; sodium / diethyl ether / 20 h / 20 °C

3.1: ethanol / 1 h / 0 - 20 °C

4.1: cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 48 h / 120 °C / Inert atmosphere

5.1: sodium hydroxide / ethanol / 2 h / 80 °C

6.1: thionyl chloride / 1 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; ethanol; sodium; magnesium; cesium fluoride; sodium hydroxide; In 1,2-dimethoxyethane; diethyl ether; ethanol; 4.1: |Suzuki Coupling;

Reference yield:

: 90326-54-8
1-(5-bromo-2-methylphenyl)ethan-1-one

: 1616930-42-7
C₁₈H₁₇N₃O₂*ClH

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol; sodium / diethyl ether / 20 h / 20 °C

2: ethanol / 1 h / 0 - 20 °C

3: cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 48 h / 120 °C / Inert atmosphere

4: sodium hydroxide / ethanol / 2 h / 80 °C

5: thionyl chloride / 1 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; ethanol; sodium; cesium fluoride; sodium hydroxide; In 1,2-dimethoxyethane; diethyl ether; ethanol; 3: |Suzuki Coupling;