5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

Base Information

Chemical Name:5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol
CAS No.:915708-08-6
Molecular Formula:C₂₆H₄₂O₆
Molecular Weight:450.616
Hs Code.:

Synonyms:5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

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Chemical Property of 5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

Chemical Property:

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Technology Process of 5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

There total 1 articles about 5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915708-07-5
2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-hex-5-enal

: 68236-10-2
3-chloromagnesiumpropan-1-olate magnesium chloride

: 915708-08-6
5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/anie.200602056

Reference yield:

: 915708-08-6
5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

: 915708-09-7
5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-4-oxo-non-8-enal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; for 0.166667h;
DOI:10.1002/anie.200602056

Reference yield:

: 915708-08-6
5-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8-(4-methoxy-benzyloxymethyl)-non-8-ene-1,4-diol

: C₃₁H₄₆O₉

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 0.17 h / -78 °C

2: aq. NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 2 h / 20 °C

3: Et₃N / tetrahydrofuran / -20 - 0 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; tert-butyl alcohol; 1: Swern oxidation / 2: Lindgren oxidation;
DOI:10.1002/anie.200602056