Technology Process of C20H21N5O6
There total 12 articles about C20H21N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium fluoride;
In
methanol;
at 60 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: trimethylsilyl trifluoromethanesulfonate; DBN / acetonitrile / 21 h / 0 - 65 °C
2.1: sodium methylate / 24 h / 20 °C
3.1: pyridine / 16 h / 20 °C
4.1: pyridine / dichloromethane / 5 h / 20 °C
5.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
6.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
6.2: 1 h / 0 °C
7.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
8.1: ammonium fluoride / methanol / 5 h / 60 °C
With
pyridine; ammonium fluoride; sodium periodate; trimethylsilyl trifluoromethanesulfonate; DBN; water; sodium methylate; sodium hydride; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; mineral oil; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / dichloromethane / 5 h / 20 °C
2.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
3.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
3.2: 1 h / 0 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
5.1: ammonium fluoride / methanol / 5 h / 60 °C
With
ammonium fluoride; sodium periodate; water; sodium hydride; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; methanol; dichloromethane; water; mineral oil; tert-butyl alcohol;