2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate
CAS No.:82462-52-0
Molecular Formula:C₂₅H₃₀O₇Si
Molecular Weight:470.595
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

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Chemical Property of 2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

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Technology Process of 2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

There total 3 articles about 2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 82462-48-4
2-(trimethylsilyl)ethyl (4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-4,5-dihydrofuran-2-carboxylate

: 82462-51-9
2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-ribo-hexonoate

: 82462-52-0
2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 48h; under 760 Torr;
DOI:10.1039/P19850000621

Reference yield:

: 23316-68-9
(2R,3R,4R,5R)-3,4-bis(benzoyloxy)-5-((benzoyloxy)methyl)tetrahydrofuran-2-carboxylic acid

: 82462-52-0
2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.) 2-chloro-N-methylpyridinium iodide, triethylamine / acetonitrile / Ambient temperature; 1.) 1.5 h, 2.) overnight

2: 34 percent / H₂ / 10percent Pd-C / ethanol / 48 h / 760 Torr

With 2-chloro-1-methyl-pyridinium iodide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1039/P19850000621

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 82462-52-0
2-(trimethylsilyl)ethyl 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino-hexonoate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.) 2-chloro-N-methylpyridinium iodide, triethylamine / acetonitrile / Ambient temperature; 1.) 1.5 h, 2.) overnight

2: 34 percent / H₂ / 10percent Pd-C / ethanol / 48 h / 760 Torr

With 2-chloro-1-methyl-pyridinium iodide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1039/P19850000621