(Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

Base Information

Chemical Name:(Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide
CAS No.:573986-23-9
Molecular Formula:C₄₈H₆₀N₄O₄
Molecular Weight:757.029
Hs Code.:

Synonyms:(Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

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Chemical Property of (Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

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Technology Process of (Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

There total 3 articles about (Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 573986-21-7
(Z)-3-(2,2-diphenylethylcarbamoyl)acrylic acid

: 573986-14-8
N¹-(12-aminododecyl)-N⁴-(2,2-diphenylethyl)succinamide

: 573986-23-9
(Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In chloroform;
DOI:10.1002/anie.200250745

Reference yield:

: 3963-62-0
2,2-Diphenylethylamine

: 573986-23-9
(Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / tetrahydrofuran

2: 70 percent / DMAP; EDCI*HCl / CHCl₃

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; chloroform;
DOI:10.1002/anie.200250745

Reference yield:

: 137379-56-7
4-((2,2-diphenylethyl)amino)-4-oxobutanoic acid

: 573986-23-9
(Z)-But-2-enedioic acid (2,2-diphenyl-ethyl)-amide {12-[3-(2,2-diphenyl-ethylcarbamoyl)-propionylamino]-dodecyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / SOCl₂ / CH₂Cl₂

2: 70 percent / DMAP; EDCI*HCl / CHCl₃

With dmap; thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; chloroform;
DOI:10.1002/anie.200250745