4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride

Base Information

• Chemical Name: 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride
• CAS No.: 69082-71-9
• Molecular Formula: C₂₀H₁₈ClN₂O₂*Cl
• Molecular Weight: 389.281

Synonyms:4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride

Chemical Property of 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride

Chemical Property:

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Technology Process of 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride

There total 3 articles about 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridine-4-carboxylic acid (55-22-1) → 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride (69082-71-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) thionyl chloride / 1.) HMPA, 30 min, 2.) HMPA, RT, overnight

2: dimethylformamide / 4 h / 110 °C

With thionyl chloride; In N,N-dimethyl-formamide;

DOI:10.1021/jm00366a017

Reference yield:

5-chloro-2-methoxyaniline (95-03-4) → 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride (69082-71-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) thionyl chloride / 1.) HMPA, 30 min, 2.) HMPA, RT, overnight

2: dimethylformamide / 4 h / 110 °C

With thionyl chloride; In N,N-dimethyl-formamide;

DOI:10.1021/jm00366a017

Reference yield:

N-(5-chloro-2-methoxyphenyl)-4-pyridinecarboxamide (69082-72-0) + benzyl chloride (100-44-7) → 4-<<(5-chloro-2-methoxyphenyl)amino>carbonyl>-1-(phenylmethyl)pyridinum chloride (69082-71-9)

Guidance literature:

In N,N-dimethyl-formamide; at 110 ℃; for 4h;

DOI:10.1021/jm00366a017

upstream raw materials:

N-(5-chloro-2-methoxyphenyl)-4-pyridinecarboxamide

benzyl chloride

pyridine-4-carboxylic acid

5-chloro-2-methoxyaniline

Downstream raw materials:

N-(5-chloro-2-methoxyphenyl)-1-(phenylmethyl)-4-piperidinecarboxamide

N-(5-chloro-2-methoxy-4-nitrophenyl)-1-(phenylmethyl)-4-piperidinecarboxamide

N-(4-amino-5-chloro-2-methoxyphenyl)-1-(phenylmethyl)-4-piperidinecarboxamide

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