4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine

Base Information

• Chemical Name: 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine
• CAS No.: 1241047-49-3
• Molecular Formula: C₅₇H₄₆N₆O₂
• Molecular Weight: 847.031
• Mol file: 1241047-49-3.mol

Synonyms:4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine

Chemical Property of 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine

There total 4 articles about 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-(2-(4-(2-(4-(4-nitro-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-5-nitrophenyl)-4,5-diphenyl-1H-imidazole (1241047-48-2) → 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine (1241047-49-3)

Guidance literature:

With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; for 5h; Reflux;

DOI:10.1016/j.reactfunctpolym.2010.02.004

Reference yield:

benzil (134-81-6) → 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine (1241047-49-3)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium acetate; acetic acid / 24 h / Reflux; Inert atmosphere

2: potassium carbonate / N,N-dimethyl acetamide / 12 h / 140 °C / Reflux; Inert atmosphere

3: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 5 h / Reflux

With palladium 10% on activated carbon; ammonium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl acetamide;

DOI:10.1016/j.reactfunctpolym.2010.02.004

Reference yield:

2-chloro-5-nitrobenzaldehyde (6361-21-3) → 4-(4-(2-(4-(4-amino-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-3-(4,5-diphenyl-1H-imidazol-2-yl)benzenamine (1241047-49-3)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium acetate; acetic acid / 24 h / Reflux; Inert atmosphere

2: potassium carbonate / N,N-dimethyl acetamide / 12 h / 140 °C / Reflux; Inert atmosphere

3: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 5 h / Reflux

With palladium 10% on activated carbon; ammonium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl acetamide;

DOI:10.1016/j.reactfunctpolym.2010.02.004

upstream raw materials:

BPA

2-(2-chloro-5-nitrophenyl)-4,5-diphenyl-1H-imidazole

2-(2-(4-(2-(4-(4-nitro-2-(4,5-diphenyl-1H-imidazol-2-yl)phenoxy)phenyl)propan-2-yl)phenoxy)-5-nitrophenyl)-4,5-diphenyl-1H-imidazole

benzil