N,N'-bis(salicylaldehyde)-1,3-diaminopentane

Base Information

Chemical Name:N,N'-bis(salicylaldehyde)-1,3-diaminopentane
CAS No.:219656-48-1
Molecular Formula:C₁₉H₂₂N₂O₂
Molecular Weight:310.396
Hs Code.:

Synonyms:N,N'-bis(salicylaldehyde)-1,3-diaminopentane

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Chemical Property of N,N'-bis(salicylaldehyde)-1,3-diaminopentane

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Technology Process of N,N'-bis(salicylaldehyde)-1,3-diaminopentane

There total 1 articles about N,N'-bis(salicylaldehyde)-1,3-diaminopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-02-8
salicylaldehyde

: 589-37-7
1,3-diaminopentane

: 219656-48-1
N,N'-bis(salicylaldehyde)-1,3-diaminopentane

Guidance literature:: for 2h; Reflux;
DOI:10.1016/j.ica.2011.06.024

Reference yield: 83.0%

: zinc(II) nitrate hexahydrate

: 219656-48-1
N,N'-bis(salicylaldehyde)-1,3-diaminopentane

: 1934-75-4
sodium dicyanamide

: [Zn2(N,N'-bis(salicylidene)-1,3-diaminopentane-2H)(μ-dicyanamide-κN1κN5)2](n)

Guidance literature:: In methanol; water; solns. of Zn-salt and diaminopentane deriv. in MeOH mixed under stirring, aq. soln. of NaN(CN)2 added, mixt. stirred for 15 min with gentle warming; soln. filtered, filtrate stored at room temp. overnight, crystals filtered off, dried in air; elem. anal.;
DOI:10.1246/bcsj.20100290

Reference yield: 82.0%

: nickel(II) perchlorate hexahydrate

: 219656-48-1
N,N'-bis(salicylaldehyde)-1,3-diaminopentane

: 65-85-0,8013-63-6
benzoic acid

: [Ni₃(N,N'-bis(salicylidene)-1,3-pentanediamine^(1-))2(benzoate)2]

Guidance literature:: With triethylamine; In methanol; MeOH soln. of bis-salicylidene deriv. added to to MeOH soln. of Ni(ClO4)2; stirred to 10 min; MeOH soln. of benzoic acid added; triethylamine added dropwise; filtered; washed with Et2O; redissolved in CH2Cl2; layered with EtOH; elem. anal.;
DOI:10.1016/j.poly.2009.07.014