methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

Base Information

Chemical Name:methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate
CAS No.:1290056-40-4
Molecular Formula:C₂₄H₃₀N₂O₆
Molecular Weight:442.512
Hs Code.:

Synonyms:methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

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Chemical Property of methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

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Technology Process of methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

There total 5 articles about methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: methyl 3-(4-(amino methyl)phenoxy)propionate

: 33233-67-9
4-(tert-Butoxycarbonylaminomethyl)benzoic acid

: 1290056-40-4
methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 1290056-40-4
methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / 1,4-dioxane / 16 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 149505-94-2
tert-butyl (4-hydroxybenzyl)carbamate

: 1290056-40-4
methyl 3-(4-((4-((tert-butoxycarbonylamino)methyl)benzamido) methyl)phenoxy)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium; hydroquinone / 48 h / Inert atmosphere; Reflux

2: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With sodium; N-ethyl-N,N-diisopropylamine; hydroquinone; HATU; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;