1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

Base Information

Chemical Name:1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide
CAS No.:134307-33-8
Molecular Formula:C₃₄H₃₇NO₇S
Molecular Weight:603.736
Hs Code.:

Synonyms:1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

Suppliers and Price of 1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

Chemical Property:

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Technology Process of 1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

There total 4 articles about 1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14233-65-9
1-N,2-O,3-O,5-O-tetrabenzyl-D-arabinonamide

: 124-63-0
methanesulfonyl chloride

: 134307-33-8
1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Yield given;
DOI:10.1002/hlca.19910740222

Reference yield:

: 14233-64-8
tri-O-benzyl-D-arabinolactone

: 134307-33-8
1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / toluene / 12 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With triethylamine; In dichloromethane; toluene;
DOI:10.1002/hlca.19910740222

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 134307-33-8
1-N,2-O,3-O,5-O-tetrabenzyl-4-O-mesyl-D-arabinonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / DMSO, Ac₂O

2: 99 percent / toluene / 12 h / Ambient temperature

3: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With acetic anhydride; dimethyl sulfoxide; triethylamine; In dichloromethane; toluene;
DOI:10.1002/hlca.19910740222