carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester

Base Information

• Chemical Name: carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester
• CAS No.: 684287-02-3
• Molecular Formula: C₂₆H₂₀FN₃O₆
• Molecular Weight: 489.46

Synonyms:carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester

Chemical Property of carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester

Chemical Property:

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Technology Process of carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester

There total 2 articles about carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

1-benzyl-6-(4-fluorobenzyl)-4,8-dihydroxy-1H-1,3,6-triaza-s-indacene-5,7-dione (684287-01-2) + chloroformic acid ethyl ester (541-41-3) → carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester (684287-02-3)

Guidance literature:

With pyridine; In N,N-dimethyl-formamide; for 16h;

DOI:10.1016/j.bmcl.2006.05.018

Reference yield: 13.0%

1-benzyl-6-(4-fluorobenzyl)-4,8-dihydroxy-1H-1,3,6-triaza-s-indacene-5,7-dione (684287-01-2) → carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester (684287-02-3)

Guidance literature:

With pyridine; ethyl hydrogen carbonate; In DMF (N,N-dimethyl-formamide); for 16h;

Reference yield: 78.0%

carbonic acid 3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester (684287-02-3) + diazodiphenylmethane (908093-98-1) → carbonic acid 8-benzhydryloxy-3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester (684287-03-4)

Guidance literature:

In 1,2-dichloro-ethane; at 70 ℃; for 24h;

DOI:10.1016/j.bmcl.2006.05.018

upstream raw materials:

1-benzyl-6-(4-fluorobenzyl)-4,8-dihydroxy-1H-1,3,6-triaza-s-indacene-5,7-dione

chloroformic acid ethyl ester

Downstream raw materials:

carbonic acid 8-benzhydryloxy-3-benzyl-6-(4-fluorobenzyl)-8-hydroxy-5,7-dioxo-3,5,6,7-tetrahydro-1,3,6-triaza-s-indacen-4-yl ester ethyl ester

4-benzhydryloxy-1-benzyl-6-(4-fluorobenzyl)-8-methoxy-1H-1,3,6-triaza-s-indacene-5,7-dione

4-benzhydryloxy-1-benzyl-6-(4-fluorobenzyl)-7-hydroxy-8-methoxy-6,7-dihydro-1H-1,3,6-triaza-s-indacen-5-one

4-benzhydryloxy-1-benzyl-6-(4-fluorobenzyl)-8-hydroxy-1H-1,3,6-triaza-s-indacene-5,7-dione

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