C₁₀H₁₁Cl₂NO₂S₃

Base Information

• Chemical Name: C₁₀H₁₁Cl₂NO₂S₃
• CAS No.: 100244-45-9
• Molecular Formula: C₁₀H₁₁Cl₂NO₂S₃
• Molecular Weight: 344.307
• Mol file: 100244-45-9.mol

Synonyms:C₁₀H₁₁Cl₂NO₂S₃

Chemical Property of C₁₀H₁₁Cl₂NO₂S₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₁₀H₁₁Cl₂NO₂S₃

There total 3 articles about C₁₀H₁₁Cl₂NO₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(methoxydichloromethyl)(chlorocarbonyl)trisulfane (88766-42-1) + N-methylaniline (100-61-8) → methyl chlorothioformate (2812-72-8) + (methylphenylcarbamoyl)disulfanyl chloride (100244-49-3) + C10H11Cl2NO2S3 (100244-45-9)

Guidance literature:

In diethyl ether; at 5 ℃; for 0.0833333h; Yields of byproduct given;

DOI:10.1021/jo00360a039

Reference yield:

N-methylaniline (100-61-8) → C10H11Cl2NO2S3 (100244-45-9)

Guidance literature:

Multi-step reaction with 2 steps

1: CDCl₃ / 22 h

2: CDCl₃

In chloroform-d1;

DOI:10.1021/jo00360a039

Reference yield:

O-methyl N-methyl-N-phenylcarbamothioate (87463-11-4) + Chlordisulfan (79598-17-7) → C10H11Cl2NO2S3 (100244-45-9)

Guidance literature:

In chloroform-d1;

DOI:10.1021/jo00360a039

upstream raw materials:

O-methyl N-methyl-N-phenylcarbamothioate

Chlordisulfan

(methoxydichloromethyl)(chlorocarbonyl)trisulfane

N-methylaniline

Downstream raw materials:

methylene chloride

(chlorocarbonyl)(methylphenylcarbamoyl)trisulfane

methyl chlorothioformate

(methylphenylcarbamoyl)disulfanyl chloride

Refernces