(chlorocarbonyl)(methylphenylcarbamoyl)trisulfane

Base Information

• Chemical Name: (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane
• CAS No.: 100244-50-6
• Molecular Formula: C₉H₈ClNO₂S₃
• Molecular Weight: 293.819
• Mol file: 100244-50-6.mol

Synonyms:(chlorocarbonyl)(methylphenylcarbamoyl)trisulfane

Chemical Property of (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane

There total 5 articles about (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H11Cl2NO2S3 (100244-45-9) → methylene chloride (74-87-3) + (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane (100244-50-6)

Guidance literature:

In chloroform-d1;

DOI:10.1021/jo00360a039

Reference yield:

(ethoxydichloromethyl)(methylphenylcarbamoyl)trisulfane (100244-46-0) → chloroethane (75-00-3) + (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane (100244-50-6)

Guidance literature:

In chloroform-d1;

DOI:10.1021/jo00360a039

Reference yield:

N-methylaniline (100-61-8) → (chlorocarbonyl)(methylphenylcarbamoyl)trisulfane (100244-50-6)

Guidance literature:

Multi-step reaction with 3 steps

1: CDCl₃ / 22 h

2: CDCl₃

3: CDCl₃

In chloroform-d1;

DOI:10.1021/jo00360a039

upstream raw materials:

C₁₀H₁₁Cl₂NO₂S₃

(ethoxydichloromethyl)(methylphenylcarbamoyl)trisulfane

bis(chlorocarbonyl)trisulfane

N-methylaniline

Downstream raw materials:

bis(methylphenylcarbamoyl)trisulfane

Refernces