benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Chemical Name:benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside
CAS No.:1309666-24-7
Molecular Formula:C₄₁H₃₈N₂O₆S
Molecular Weight:686.829
Hs Code.:

Synonyms:benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Chemical Property of benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Technology Process of benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

There total 1 articles about benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 40246-27-3
3,4,6-tri-O-benzyl-1,2-O-methoxybenzylidene-α-D-glucopyranose

: 134469-07-1
Benzimidazol-2-thiol

: 1309666-24-7
benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: 3,4,6-tri-O-benzyl-1,2-O-methoxybenzylidene-α-D-glucopyranose; In acetonitrile; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

Benzimidazol-2-thiol; With mercury dibromide; for 6h; Reflux;
DOI:10.1002/anie.201007212

Reference yield: 98.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1309666-24-7
benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: methyl O-(2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzyl-D-glucopyranoside; benzimidazol-2-yl 2-O-benzoyl-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside; In 1,2-dichloro-ethane; for 1h; Molecular sieve; Inert atmosphere;

With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 0.0833333h; Inert atmosphere;
DOI:10.1002/anie.201007212