1H-Indene, 2,3-dihydro-5-nitro-, radical ion(1-) (9CI)

Base Information

• Chemical Name: 1H-Indene, 2,3-dihydro-5-nitro-, radical ion(1-) (9CI)
• CAS No.: 34517-17-4
• Molecular Formula: C₉H₉NO₂
• Molecular Weight: 163.176
• Mol file: 34517-17-4.mol

Synonyms:1H-Indene, 2,3-dihydro-5-nitro-, radical ion(1-) (9CI)

Chemical Property of 1H-Indene, 2,3-dihydro-5-nitro-, radical ion(1-) (9CI)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1H-Indene, 2,3-dihydro-5-nitro-, radical ion(1-) (9CI)

There total 6 articles about 1H-Indene, 2,3-dihydro-5-nitro-, radical ion(1-) (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

6-(trimethylsilyl)-5-indanyl triflate → 5-nitroindane (7436-07-9,34517-17-4)

Guidance literature:

With water; cesium fluoride; sodium nitrite; In acetonitrile; at 20 ℃; for 12h;

DOI:10.1021/acs.orglett.6b01384

Reference yield: 36.0%

6-nitroindan-1-one (24623-24-3) → 5-nitroindane (7436-07-9,34517-17-4)

Guidance literature:

With triethylsilane; boron trifluoride diethyl etherate; at 20 ℃;

DOI:10.1002/chem.201904930

Reference yield:

INDANE (496-11-7) → 4-nitroindane (34701-14-9) + 5-nitroindane (7436-07-9,34517-17-4)

Guidance literature:

With sulfuric acid; nitric acid; at -10 ℃;

DOI:10.1021/ja01850a049

upstream raw materials:

INDANE

6-nitroindan-1-one