9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate

Base Information

• Chemical Name: 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate
• CAS No.: 1378318-52-5
• Molecular Formula: C₂₄H₁₁F₇Hg₂O₇
• Molecular Weight: 945.516
• Mol file: 1378318-52-5.mol

Synonyms:9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate

Chemical Property of 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate

There total 4 articles about 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

9-(4-fluorophenyl)-6-methoxy-3-fluorone (1378318-46-7) + trifluoroacetic acid (76-05-1) + mercury(II) oxide (12653-71-3) → 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate (1378318-52-5)

Guidance literature:

at 20 ℃;

Reference yield:

1-Bromo-2,4-dimethoxybenzene (17715-69-4) → 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate (1378318-52-5)

Guidance literature:

Multi-step reaction with 3 steps

1: iodine; magnesium / tetrahydrofuran / 0.5 h

2: boron tribromide / dichloromethane / -78 °C

3: 20 °C

With iodine; boron tribromide; magnesium; In tetrahydrofuran; dichloromethane;

Reference yield:

methyl 4-flurobenzoate (403-33-8) → 9-(4-fluorophenyl)-6-methoxy-3-fluorone-2,5-dimercuric trifluoroacetate (1378318-52-5)

Guidance literature:

Multi-step reaction with 3 steps

1: iodine; magnesium / tetrahydrofuran / 0.5 h

2: boron tribromide / dichloromethane / -78 °C

3: 20 °C

With iodine; boron tribromide; magnesium; In tetrahydrofuran; dichloromethane;

upstream raw materials:

9-(4-fluorophenyl)-6-methoxy-3-fluorone

trifluoroacetic acid

mercury(II) oxide

1-Bromo-2,4-dimethoxybenzene