1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene

Base Information

Chemical Name:1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene
CAS No.:1344700-08-8
Molecular Formula:C₁₅H₁₉IN₂O₄
Molecular Weight:418.231
Hs Code.:

Synonyms:1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene

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Technology Process of 1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene

There total 2 articles about 1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1344700-05-5
O-ethyl-N,N²,2-trimethyl-3-oxoserinamide

: 1711-02-0
4-iodobenzoic acid chloride

: 1344700-08-8
1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 0.666667h; Cooling with ice;

Reference yield:

: 29263-94-3
diethyl bromomethylmalonate

: 1344700-08-8
1-{[1-ethoxy-2-methyl-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}-4-iodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 16 h / 20 °C / Cooling with ice

2: N-ethyl-N,N-diisopropylamine / chloroform / 0.67 h / 20 °C / Cooling with ice

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform;