3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

Base Information

Chemical Name:3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one
CAS No.:1450627-70-9
Molecular Formula:C₁₅H₁₈N₄O₃
Molecular Weight:302.333
Hs Code.:

Synonyms:3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

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Chemical Property of 3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

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Technology Process of 3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

There total 6 articles about 3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1450627-90-3
C₁₄H₁₆N₄O₃

: 1450627-70-9
3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

Guidance literature:: With hydrogenchloride; In water; at 20 ℃; for 6h;
DOI:10.1016/j.bmc.2013.06.069

Reference yield:

: 67-56-1
methanol

: 1450627-88-9
5-amino-1-(4-methoxybenzyl)-N-(2,2'-dimethoxy ethyl)-1H-imidazole-4-carboxamide

: 1450627-70-9
3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

Guidance literature:: With hydrogenchloride; water; at 50 ℃; for 24h;
DOI:10.1016/j.bmc.2013.06.069

Reference yield:

: 1450627-80-1
1-(4-methoxybenzyl)-5-nitro-4-styryl-1H-imidazole

: 1450627-70-9
3-(4-methoxybenzyl)-5-methoxy-4,5,6,7-tetrahydro imidazo[4,5-e][1,4]diazepin-8(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; potassium permanganate / water / 0 - 5 °C

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / Reflux; Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / methanol / 5 h / 2844.39 Torr

4.1: hydrogenchloride; water / 24 h / 50 °C

With hydrogenchloride; potassium permanganate; palladium on activated charcoal; water; hydrogen; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2013.06.069