TH₀₄₃₀₆-003

Base Information

Chemical Name:TH₀₄₃₀₆-003
CAS No.:1431960-86-9
Molecular Formula:C₁₅H₁₈N₂O₂S
Molecular Weight:290.386
Hs Code.:

Synonyms:TH₀₄₃₀₆-003

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TH₀₄₃₀₆-003

Chemical Property:

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Technology Process of TH₀₄₃₀₆-003

There total 4 articles about TH₀₄₃₀₆-003 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.6%

: 905300-76-7
tert-butyl (2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)carbamate

: 34259-99-9
4-bromo-1,3-thiazole

: 1431960-86-9
TH₀₄₃₀₆-003

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; at 120 ℃; for 0.5h; Microwave irradiation; Inert atmosphere;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1431960-86-9
TH₀₄₃₀₆-003

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 20 °C

2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

3: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 0.5 h / 120 °C / Microwave irradiation; Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; potassium carbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 162356-90-3
N-(tert-butoxycarbonyl)-2-bromobenzylamine

: 1431960-86-9
TH₀₄₃₀₆-003

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 0.5 h / 120 °C / Microwave irradiation; Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; potassium carbonate; In 1,4-dioxane; water; N,N-dimethyl-formamide;