(hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

Base Information

Chemical Name:(hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle
CAS No.:100935-63-5
Molecular Formula:C₁₈H₁₈O₆
Molecular Weight:330.337
Hs Code.:

Synonyms:(hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

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Chemical Property of (hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

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Technology Process of (hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

There total 5 articles about (hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 100935-58-8
phenacyl-3 hydroxy-6 phthalate de methyle

: 100935-63-5
(hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

Guidance literature:: With potassium borohydride; In methanol; for 2h; Heating;
DOI:10.1002/jhet.5570220361

Reference yield:

: 24954-15-2
phenacyl-2 furanne

: 100935-63-5
(hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 8 h / Heating

2: 90 percent / BF₃*Et₂O / CH₂Cl₂ / 0.5 h

3: 70 percent / KBH₄ / methanol / 2 h / Heating

With potassium borohydride; boron trifluoride diethyl etherate; In methanol; dichloromethane; benzene;
DOI:10.1002/jhet.5570220361

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 100935-63-5
(hydroxy-2 phenyl-2 ethyl)-3 hydroxy-6 phthalate de methyle

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / ZnCl₂ / acetic acid / 0.5 h / Heating

2: 86 percent / LiCl/N-methylpyrolidone / acetic acid / 5 h / Heating

3: benzene / 8 h / Heating

4: 90 percent / BF₃*Et₂O / CH₂Cl₂ / 0.5 h

5: 70 percent / KBH₄ / methanol / 2 h / Heating

With 1-methyl-pyrrolidin-2-one; potassium borohydride; boron trifluoride diethyl etherate; lithium chloride; zinc(II) chloride; In methanol; dichloromethane; acetic acid; benzene;
DOI:10.1002/jhet.5570220361