α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

Base Information

Chemical Name:α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide
CAS No.:1241896-20-7
Molecular Formula:Br*C₁₇H₂₈OP
Molecular Weight:359.286
Hs Code.:

Synonyms:α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

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Chemical Property of α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

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Technology Process of α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

There total 1 articles about α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 15647-86-6
triethylphosphine hydrobromide

: 137032-32-7
α-methyl-trans-cinnamaldehyde dimethyl acetal

: 1241896-20-7
α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

Guidance literature:: at 80 ℃; for 0.833333h; Inert atmosphere; neat (no solvent);
DOI:10.1002/ejoc.201000601

Reference yield:

: 1241896-20-7
α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

: C₁₇H₂₇OP

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.07.083

Reference yield:

: 1241896-20-7
α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide

: 123-11-5
4-methoxy-benzaldehyde

: 1241896-35-4
(E,E)-1-(p-methoxyphenyl)-2-methoxy-3-methyl-4-phenyl-1,3-butadiene

: (1Z,3E)-1-(p-methoxyphenyl)-2-methoxy-3-methyl-4-phenyl-1,3-butadiene

Guidance literature:: α-methoxy-triethyl[(2E)-2-methyl-3-phenyl-2-propenyl]phosphonium bromide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.583333h; Inert atmosphere;

4-methoxy-benzaldehyde; In tetrahydrofuran; at 0 - 20 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201000601