C₁₀H₁₁NO₄

Base Information

• Chemical Name: C₁₀H₁₁NO₄
• CAS No.: 1360446-25-8
• Molecular Formula: C₁₀H₁₁NO₄
• Molecular Weight: 209.202
• Mol file: 1360446-25-8.mol

Synonyms:C₁₀H₁₁NO₄

Chemical Property of C₁₀H₁₁NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₁NO₄

There total 3 articles about C₁₀H₁₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

C10H9NO4 (914769-85-0) → C10H11NO4 (1360446-25-8)

Guidance literature:

With sodium tetrahydroborate; silica gel; In chloroform; isopropyl alcohol; at 0 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c2cc17458h

Reference yield:

3-nitro-4-(2-propenyloxy)benzaldehyde (125872-98-2) → C10H11NO4 (1360446-25-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 17 h / 160 - 165 °C / Inert atmosphere

2: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol / 1 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; silica gel; In chloroform; isopropyl alcohol; 1: Claisen rearrangement;

DOI:10.1039/c2cc17458h

Reference yield:

4-hydroxy-3-nitrobenzaldehyde (3011-34-5) → C10H11NO4 (1360446-25-8)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 72 h / 60 °C / Inert atmosphere

2: 17 h / 160 - 165 °C / Inert atmosphere

3: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol / 1 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; silica gel; potassium carbonate; In chloroform; isopropyl alcohol; acetonitrile; 2: Claisen rearrangement;

DOI:10.1039/c2cc17458h

upstream raw materials:

C₁₀H₉NO₄

4-hydroxy-3-nitrobenzaldehyde

3-nitro-4-(2-propenyloxy)benzaldehyde