4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

Base Information

Chemical Name:4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile
CAS No.:1264751-92-9
Molecular Formula:C₂₃H₁₇N₃O₃S
Molecular Weight:415.472
Hs Code.:

Synonyms:4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

There total 3 articles about 4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1264754-24-6
4-(4-{hydroxy[4-(methylamino)-2-oxo-2,5-dihydro-1,3-thiazol-5-yl]methyl}-2-methoxyphenoxy)naphthalene-1-carbonitrile

: 1264751-92-9
4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

Guidance literature:: 4-(4-{hydroxy[4-(methylamino)-2-oxo-2,5-dihydro-1,3-thiazol-5-yl]methyl}-2-methoxyphenoxy)naphthalene-1-carbonitrile; With hydrogenchloride; In ethyl acetate; for 2h; Reflux;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1264751-92-9
4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium carbonate / dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 48 h / 100 °C

2.1: potassium tert-butylate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride / ethyl acetate / 2 h / Reflux

With hydrogenchloride; potassium tert-butylate; lithium carbonate; In dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 13916-99-9
4-fluoronaphthalene-1-carbonitrile

: 1264751-92-9
4-(2-methoxy-4-{(Z)-[4-(methylamino)-2-oxo-1,3-thiazol-5(2H)-ylidene]methyl}phenoxy)naphthalene-1-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium carbonate / dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 48 h / 100 °C

2.1: potassium tert-butylate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride / ethyl acetate / 2 h / Reflux

With hydrogenchloride; potassium tert-butylate; lithium carbonate; In dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;