diethyl bismuth ⁽¹⁺⁾; diethyl bismuth bromide

Base Information

• Chemical Name: diethyl bismuth ⁽¹⁺⁾; diethyl bismuth bromide
• CAS No.: 54291-01-9
• Molecular Formula: C₄H₁₀BiBr
• Molecular Weight: 347.008

Synonyms:diethyl bismuth ⁽¹⁺⁾; diethyl bismuth bromide

Chemical Property of diethyl bismuth ⁽¹⁺⁾; diethyl bismuth bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diethyl bismuth ⁽¹⁺⁾; diethyl bismuth bromide

There total 1 articles about diethyl bismuth ⁽¹⁺⁾; diethyl bismuth bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylbismuth (617-77-6) → ethyl bromide (74-96-4) + diethyl bismuth (1+); diethyl bismuth bromide (54291-01-9)

Guidance literature:

With Br₂; In petroleum ether; cooling;

Reference yield: 76.0%

styrene oxide (96-09-3) + sodium (7440-23-5) + diethyl bismuth (1+); diethyl bismuth bromide (54291-01-9) → diethyl-(2-hydroxy-2-phenyl)ethylbismuthane (169052-37-3)

Guidance literature:

With water; In ammonia; byproducts: NaBr; Ar atm.; 2 equiv. of Na, cooling (-78°C, absence of light), stirring (15 min, -78°C), heating (to -50°C); evapn. (-30 to 0°C), extraction (0°C, Et2O/C6H6/H2O 5:1:2), filtn., drying (MgSO4), evapn. (vac., 0°C); elem. anal.;

upstream raw materials:

triethylbismuth

Downstream raw materials:

diethyl-(2-hydroxy-2-phenyl)ethylbismuthane

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