9-phenyl-10,9-oxaboraphenanthrene

Base Information Edit

Chemical Name:9-phenyl-10,9-oxaboraphenanthrene
CAS No.:19374-73-3
Molecular Formula:C₁₈H₁₃BO
Molecular Weight:256.112
Hs Code.:
Mol file:19374-73-3.mol

Synonyms:9-phenyl-10,9-oxaboraphenanthrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-phenyl-10,9-oxaboraphenanthrene Edit

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Technology Process of 9-phenyl-10,9-oxaboraphenanthrene

There total 17 articles about 9-phenyl-10,9-oxaboraphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 19091-73-7
9-chloro-9-bora-10-oxa-phenanthrene

: 591-51-5
phenyllithium

: C₂₄H₁₈BO^(1-)*Li⁽¹⁺⁾

: 19374-73-3
9-phenyl-10,9-oxaboraphenanthrene

Guidance literature:: In tetrahydrofuran; dibutyl ether; for 2.5h; Inert atmosphere; Cooling;
DOI:10.1016/j.tet.2016.01.054

Reference yield:

: 90-43-7,287950-96-3
2-Phenylphenol

: 19374-73-3
9-phenyl-10,9-oxaboraphenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: (i) BCl₃, CH₂Cl₂, (ii) AlCl₃, PE

2: benzene

In benzene;
DOI:10.1039/jr9600001344