N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide

Base Information

Chemical Name:N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide
CAS No.:664351-10-4
Molecular Formula:C₁₂H₁₄N₄O
Molecular Weight:230.269
Hs Code.:
DSSTox Substance ID:DTXSID601180188

Synonyms:DTXSID601180188;664351-10-4;N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide

Suppliers and Price of N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:230.11676108
Heavy Atom Count:17
Complexity:265

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(N=NN1CC2=CC=CC=C2)C(=O)NC

Technology Process of N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide

There total 3 articles about N,5-Dimethyl-1-(phenylmethyl)-1H-1,2,3-triazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 74-89-5
methylamine

: 664351-09-1
1-benzyl-5-methyl-1H-1,2,3-triazol-4-carbonyl chloride

: 664351-10-4
1-benzyl-5-methyl-4-(N-methyl)carboxamido-1H-1,2,3-triazole

Guidance literature:: In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2003.09.003

Reference yield:

: 54698-60-1
1-benzyl-5-methyl-1H-1,2,3-triazole-4-carboxylic acid

: 664351-10-4
1-benzyl-5-methyl-4-(N-methyl)carboxamido-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 3 h / Heating

2: 92 percent / H₂O; tetrahydrofuran / 24 h / 20 °C

With thionyl chloride; In tetrahydrofuran; water;
DOI:10.1016/j.ejmech.2003.09.003

Reference yield:

: 133992-58-2
1-benzyl-5-methyl-1H-1,2,3-triazol-4-carboxylic acid ethyl ester

: 664351-10-4
1-benzyl-5-methyl-4-(N-methyl)carboxamido-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / 2 h / Heating

2: SOCl₂ / 3 h / Heating

3: 92 percent / H₂O; tetrahydrofuran / 24 h / 20 °C

With sodium hydroxide; thionyl chloride; In tetrahydrofuran; water;
DOI:10.1016/j.ejmech.2003.09.003