(N-Methyl-N-phenylamino)triphenylphosphonium Iodide

Base Information

• Chemical Name: (N-Methyl-N-phenylamino)triphenylphosphonium Iodide
• CAS No.: 34257-63-1
• Molecular Formula: C25H23 N P . I
• Molecular Weight: 495.343
• European Community (EC) Number: 672-690-7
• DSSTox Substance ID: DTXSID20385189
• Mol file: 34257-63-1.mol

Synonyms:(N-Methyl-N-phenylamino)triphenylphosphonium Iodide;34257-63-1;(N-methylanilino)-triphenylphosphanium;iodide;(Methyl(phenyl)amino)triphenylphosphonium iodide;SCHEMBL3421857;DTXSID20385189;SAYKZWPCENNSDR-UHFFFAOYSA-M;MFCD00040544;AKOS015833274;N-Methylanilinotriphenylphosphonium Iodide;CS-0451373;FT-0639174;M1151;(Methyl(phenyl)amino)triphenylphosphoniumiodide;D91450;N-methyl-N-phenylaminotriphenylphosphonium iodide;J-019526;Phosphorus(1+), (N-methylbenzenaminato)triphenyl-, iodide, (T-4)-

Chemical Property of (N-Methyl-N-phenylamino)triphenylphosphonium Iodide

Chemical Property:

• Melting Point: 238-239°C
• PSA: 16.83000
• LogP: 2.03590
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 495.06128
• Heavy Atom Count: 28
• Complexity: 380

Purity/Quality:

98%,99%, ^*data from raw suppliers

(N-Methyl-N-phenylamino)triphenylphosphonium Iodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.
• Hazard Codes: R36/37/38:Irritating to eyes, respiratory system and skin.
• Statements: 36/37/38
• Safety Statements: 26-36-24/25-22

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C1=CC=CC=C1)[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4.[I-]

Technology Process of (N-Methyl-N-phenylamino)triphenylphosphonium Iodide

There total 3 articles about (N-Methyl-N-phenylamino)triphenylphosphonium Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-phenyltriphenyliminophosphorane (2325-27-1) + methyl iodide (74-88-4) → N-methyl-N-phenylaminotriphenylphosphonium iodide (34257-63-1)

Guidance literature:

In benzene; for 8h; Heating;

DOI:10.1055/s-1980-28997

Reference yield:

triphenylphosphine (603-35-0) → N-methyl-N-phenylaminotriphenylphosphonium iodide (34257-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 0.5 h / Heating

2: benzene / 2 h / Heating

In benzene;

Reference yield:

Phenyl azide (622-37-7) → N-methyl-N-phenylaminotriphenylphosphonium iodide (34257-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 0.5 h / Heating

2: benzene / 2 h / Heating

In benzene;

upstream raw materials:

N-phenyltriphenyliminophosphorane

methyl iodide

triphenylphosphine

Phenyl azide

Downstream raw materials:

N-methylaniline

iodure de triphenyl N,N-dimethylaminophosphonium

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