N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

Base Information

Chemical Name:N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine
CAS No.:1314097-34-1
Molecular Formula:C₂₈H₄₃N₅O₈
Molecular Weight:577.678
Hs Code.:

Synonyms:N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

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Chemical Property of N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

Chemical Property:

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Technology Process of N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

There total 5 articles about N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1314097-19-2
methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

: 1314097-34-1
N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 60 ℃; for 0.05h; sealed tube; Microwave irradiation;
DOI:10.1039/c1ob05471f

Reference yield:

: 1314097-03-4
methyl N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycinate

: 1314097-34-1
N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

Guidance literature:: Multi-step reaction with 3 steps

1: water; lithium hydroxide / tetrahydrofuran / 0.05 h / 60 °C / sealed tube; Microwave irradiation

2: sodium sulfate / 0.08 h / 45 °C / sealed tube; Microwave irradiation; neat (no solvent)

3: water; lithium hydroxide / tetrahydrofuran / 0.05 h / 60 °C / sealed tube; Microwave irradiation

With water; sodium sulfate; lithium hydroxide; In tetrahydrofuran; 2: Ugi reaction;
DOI:10.1039/c1ob05471f

Reference yield:

: 1314097-12-5
N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycine

: 1314097-34-1
N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / 0.08 h / 45 °C / sealed tube; Microwave irradiation; neat (no solvent)

2: water; lithium hydroxide / tetrahydrofuran / 0.05 h / 60 °C / sealed tube; Microwave irradiation

With water; sodium sulfate; lithium hydroxide; In tetrahydrofuran; 1: Ugi reaction;
DOI:10.1039/c1ob05471f